74497-02-2合成路线 (共 11739 条)
参考文献
Simonov, V. D.; Chernova, L. N.; Akhmerova, S. G.; Yasman, Ya. B.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 1974 - 1978
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 11 p. 2313 - 2318
反应条件
2: alcoholic NaOH-solution
View Scheme
参考文献
Zincke; Ruppersberg
Chemische Berichte, 1915 , vol. 48, p. 123
反应条件
1: With [Pd(dppe)(H2O)2](TfO)2 in 1,4-dioxane
T=80°C; 24 h;
2: With silica gel in dichloromethane
T=20°C; 2 h;
参考文献
Shimada, Tomohiro; Bajracharya, Gan B.; Yamamoto, Yoshinori
European Journal of Organic Chemistry, 2005 , # 1 p. 59 - 62
反应条件
in dichloromethane
T=20°C; 18 h; Inert atmosphereMolecular sieve;
参考文献
Arrowsmith, Merle; Hill, Michael S.; Kociok-Koehn, Gabriele
Chemistry - A European Journal, 2013 , vol. 19, # 8 p. 2776 - 2783
参考文献
Bachmann; Cronyn
Chem.Penicillin, <Princeton 1949>, S. 849,871
Full Text Show Details
Cornforth
Chem.Penicillin, <Princeton 1949>, S. 688,783
参考文献
Lur'e et al.
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 1308,1310; engl. Ausg. S. 1431, 1433
反应条件
1: zinc chloride / Verseifen des Reaktionsprodukts mit Salzsaeure
2: sodium carbonate; diethyl ether
View Scheme
参考文献
Raadsveld
Recueil des Travaux Chimiques des Pays-Bas, 1935 , vol. 54, p. 813,824
反应条件
1: benzene-1,2,4,5-tetracarboxylic acid With 2,6-bis[(2,2,6,6-tetramethylpiperidin-1-yl)methyl]phenylboronic acid in n-butyronitrile
12 h; Reflux;
2: aniline in n-butyronitrile
T=20°C; 3 h;
参考文献
NATIONAL UNIVERSITY CORPORATION NAGOYA UNIVERSITY
Patent: US2011/319620 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
in N,N-dimethyl-formamide
参考文献
Sakakura, Akira; Ohkubo, Takuro; Yamashita, Risa; Akakura, Matsujiro; Ishihara, Kazuaki
Organic Letters, 2011 , vol. 13, # 5 p. 892 - 895
反应条件
aniline hydrochloric acid
T=160 - 170°C;
参考文献
Bayer and Co.
Patent: DE70349 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 3, p. 513