74497-02-2合成路线 （共 11739 条）
反应条件
1: 4-methylbenzenesulfonic acid N-methylidene-hydrazide With sodium hydride in toluene
T=0 - 20°C; 0.5 h; Inert atmosphere;
2: carbon monoxide; aniline With tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene
T=60°C; P=760.051 Torr; 24 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
反应条件
potassium phosphate; 5,10,15,20-tetraphenyl-21H,23H-porphine Co(II); Aliquat® 336 in toluene
T=50°C; P=7500.75 Torr; 18 h; Inert atmosphereAutoclave; Reagent/catalystSolvent;
参考文献
Paul, Nanda D.; Chirila, Andrei; Lu, Hongjian; Zhang, X. Peter; Debruin, Bas
Chemistry - A European Journal, 2013 , vol. 19, # 39 p. 12953 - 12958
反应条件
1: benzaldehyde With sodium sulfate; toluene-4-sulfonic acid hydrazide in toluene
T=60°C; 0.0833333 h; Inert atmosphere;
2: carbon monoxide; aniline With tris-(dibenzylideneacetone)dipalladium(0); lithium tert-butylate in toluene
T=60°C; P=760.051 Torr; 23 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
反应条件
di-tert-butyl peroxide; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; palladium dichloride
T=125°C; P=38002.6 Torr; 24 h; Autoclave; Reagent/catalystTemperature;
参考文献
Liu, Huizhen; Laurenczy, Gabor; Yan, Ning; Dyson, Paul J.
Chemical Communications, 2014 , vol. 50, # 3 p. 341 - 343
反应条件
CAL-B in tert-butyl methyl ether
T=55°C; 8 h; Green chemistryEnzymatic reaction; chemoselective reaction;
参考文献
Lal, Samridhi; Snape, Timothy J.
RSC Advances, 2014 , vol. 4, # 4 p. 1609 - 1615
反应条件
1: T=100 - 130°C;
2: With caesium carbonate in 1,4-dioxane
T=100°C;
参考文献
Mahajan, Pankaj S.; Mahajan, Jyoti P.; Mhaske, Santosh B.
Synthetic Communications, 2013 , vol. 43, # 18 p. 2508 - 2516
反应条件
1: phenylacetic acid; diethyl chlorophosphate With triethylamine in tetrahydrofuran
T=15 - 20°C; 3 h;
2: aniline in tetrahydrofuran
T=20 - 25°C; 1 h;
参考文献
Gaede, Bruce
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 92 - 93
反应条件
potassium tert-butylate; Aliquatreg; 336
T=150°C; 0.0333333 h; microwave irradiation;
参考文献
Perreux, Laurence; Loupy, Andre; Delmotte, Michel
Tetrahedron, 2003 , vol. 59, # 12 p. 2185 - 2189
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=110°C; P=15514.9 Torr; 15 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
反应条件
palladium diacetate; triphenylphosphine in tetrahydrofuran
T=110°C; P=15514.9 Torr; 10 h;
参考文献
Troisi, Luigino; Granito, Catia; Rosato, Francesca; Videtta, Valeria
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 371 - 373
