74497-02-2合成路线 (共 11739 条)
反应条件
in N,N-dimethyl-formamide 2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
in N,N-dimethyl-formamide T=80°C; 0.5 h;
参考文献
Umemoto, Teruo; Ishihara, Sumi; Adachi, Kenji
Journal of Fluorine Chemistry, 1995 , vol. 74, # 1 p. 77 - 82
反应条件
in N,N-dimethyl-formamide T=80°C; 7 h;
参考文献
Umemoto, Teruo; Ishihara, Sumi; Adachi, Kenji
Journal of Fluorine Chemistry, 1995 , vol. 74, # 1 p. 77 - 82
反应条件
in DMF-d7 T=62°C; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Ono, Taizo; Umemoto, Teruo
Journal of Fluorine Chemistry, 1996 , vol. 80, # 2 p. 163 - 166
反应条件
in DMF-d7 T=-10°C; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Ono, Taizo; Umemoto, Teruo
Journal of Fluorine Chemistry, 1996 , vol. 80, # 2 p. 163 - 166
反应条件
in DMF-d7 T=81.4°C; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Ono, Taizo; Umemoto, Teruo
Journal of Fluorine Chemistry, 1996 , vol. 80, # 2 p. 163 - 166
参考文献
Wieland; Jung
Justus Liebigs Annalen der Chemie, 1925 , vol. 445, p. 86
参考文献
Wieland; Jung
Justus Liebigs Annalen der Chemie, 1925 , vol. 445, p. 86
反应条件
1: pyridine / ethyl acetate / 3 h / 0 - 20 °C 2: hydrazine hydrate / ethylene glycol dimethyl ether / 24 h / 20 °C View Scheme
参考文献
Kashaw, Sushil K.; Kashaw, Varsha; Mishra, Pradeep; Jain; Stables
Medicinal Chemistry Research, 2011 , vol. 20, # 6 p. 738 - 745
反应条件
und Spaltung des entstandenen Aceton-phenylsemicarbazons mit siedender verd.Salzsaeure;
参考文献
Borsche
Chemische Berichte, 1905 , vol. 38, p. 833