74497-02-2合成路线 （共 11739 条）
反应条件
potassium tert-butylate; (π-allyl)(diphosphinecyclobutene)palladium in toluene T=20°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 69, # 19 p. 6504 - 6506
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0) in toluene T=105°C; 24 h;
参考文献
Journal of Organic Chemistry, , vol. 68, # 25 p. 9563 - 9573
反应条件
1: 77 percent / ethanol / Heating 2: 51 percent / NaBO3*4H2O / trifluoroacetic acid / Heating View Scheme
参考文献
Nongkunsarn, Pakawan; Ramsden, Christopher A.
Tetrahedron, 1997 , vol. 53, # 10 p. 3805 - 3830
反应条件
potassium carbonate in water T=20°C;
参考文献
Sawant, Sanghapal D.; Srinivas, Mahesuni; Aravinda Kumar; Lakshma Reddy; Singh, Parvinder Pal; Singh, Baldev; Sharma, Amit Kumar; Sharma; Vishwakarma, Ram A.
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5351 - 5354
反应条件
sodium t-butanolate; Pd catalyst in toluene T=110°C; Arylation; 2 h;
参考文献
Martin, Juliette; Marriere, Eddie; Perrio-Huard, Cecile; Barre, Louisa; Lasne, Marie Claire
Journal of Labelled Compounds and Radiopharmaceuticals, 1998 , vol. 41, # 11 p. 1042 - 1044
反应条件
caesium carbonate; palladium diacetate in toluene T=100°C; 38 h;
参考文献
Oishi, Shinya; Watanabe, Toshiaki; Sawada, Jun-Ichi; Asai, Akira; Ohno, Hiroaki; Fujii, Nobutaka
Journal of Medicinal Chemistry, 2010 , vol. 53, # 13 p. 5054 - 5058
反应条件
1: aniline With copper diacetate in acetonitrile T=-5°C; 0.25 h; 2: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in acetonitrile T=-5°C; 0.0833333 h; 3: 4-fluoro-phenylhydrazine in acetonitrile T=-5°C; 3.33333 h;
参考文献
Jadhav, Ravindra R.; Huddar, Sameerana N.; Akamanchi, Krishnacharya G.
European Journal of Organic Chemistry, 2013 , # 30 p. 6779 - 6783
反应条件
1.1: copper(l) chloride; potassium carbonate / 1,2-dichloro-benzene / 15 h / 170 °C 1.2: 2 h 2.1: sulfuric acid / 12 h / |Reflux 3.1: pyridine / chloroform / 4 h / 20 - 80 °C 4.1: potassium hydroxide; methanol / 15 h / 20 °C 5.1: sulfuric acid / water / 8 h / 20 °C 6.1: hydrazine hydrate / ethanol; diethylene glycol / 8 h / |Reflux 6.2: 5 h / |Reflux View Scheme
参考文献
Australian Journal of Chemistry, , vol. 66, # 6 p. 635 - 645
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in 1,4-dioxane T=150°C; 5 h;
参考文献
Abbenhuis; Boersma; Van Koten
Journal of Organic Chemistry, 1998 , vol. 63, # 13 p. 4282 - 4290
反应条件
potassium carbonate in ethanol; water T=120°C; P=3878.71 Torr; 0.0833333 h;
参考文献
He, Hongjie; Lin, Qi; Liu, Xiaofeng; Yang, Yongtai; Zhou, Yaming; Jia, Yu; Gao, Xiang
Synthetic Communications, 2012 , vol. 42, # 17 p. 2512 - 2525
