74497-02-2合成路线 （共 11739 条）
反应条件
sodium lauryl sulfate; sodium hydrogencarbonate in water T=80°C; 1 h; Inert atmosphere;
参考文献
Shu, Xing-Zhong; Yang, Yan-Fang; Xia, Xiao-Feng; Ji, Ke-Gong; Liu, Xue-Yuan; Liang, Yong-Min
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4077 - 4079
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; di-n-butylchlorotin hydride in tetrahydrofuran T=0°C; Reduction; Amination; 1.5 h;
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synthesis, 2000 , # 6 p. 789 - 800
反应条件
(C6H3N(CH2NMe2)2)RuCl2(PPh3) in 1,4-dioxane T=150°C; 5 h;
参考文献
Yuan, Kedong; Jiang, Fan; Sahli, Zeyneb; Achard, Mathieu; Roisnel, Thierry; Bruneau, Christian
Angewandte Chemie - International Edition, 2012 , vol. 51, # 35 p. 8876 - 8880
反应条件
1: 1,5-dihydroxypentane; aniline With C28H29ClIrO3PS in toluene T=150°C; 16 h; Inert atmosphere; 2: benzaldehyde With D-(+)-camphor sulfonic acid in toluene T=150°C; 20 h; Inert atmosphere; 3: With formic acid in toluene T=150°C; 2 h; Inert atmosphere;
参考文献
Yuan, Kedong; Jiang, Fan; Sahli, Zeyneb; Achard, Mathieu; Roisnel, Thierry; Bruneau, Christian
Angewandte Chemie - International Edition, 2012 , vol. 51, # 35 p. 8876 - 8880
反应条件
aluminum oxide T=300°C;
参考文献
Hargis, Duane C.; Shubkin, Ronald L.
Tetrahedron Letters, 1990 , vol. 31, # 21 p. 2991 - 2994
参考文献
Scriabine
Bulletin de la Societe Chimique de France, 1947 , p. 454
参考文献
Hallas, Geoffrey; Marsden, Richard; Hepworth, John D.; Mason, Donald
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 1 p. 149 - 154
反应条件
[Pd(cinnamyl)Cl]2; 2-(di-1-adamantylphosphino)-N,N-dimethylaniline; sodium t-butanolate in toluene 1 h; chemoselective reaction;
参考文献
Lundgren, Rylan J.; Sappong-Kumankumah, Antonia; Stradiotto, Mark
Chemistry - A European Journal, 2010 , vol. 16, # 6 p. 1983 - 1991
反应条件
T=130 - 140°C; man loest das erkaltete Produkt in kochendem Wasser und traegt allmaehlich in siedende verd.Schwefelsaeure;
参考文献
Laurent; Gerhardt
Annales de Chimie (Cachan, France), 1848 , vol. <3>24, p. 166
Justus Liebigs Annalen der Chemie, 1848 , vol. 68, p. 18
反应条件
1: Et3N / CH2Cl2 / 1 h / 0 - 20 °C 2: aq. LiOH / dioxane / 1 h / 20 °C View Scheme
参考文献
Sit, Sing-Yuen; Ehrgott, Frederick J.; Gao, Jinnian; Meanwell, Nicholas A.
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 5 p. 499 - 504
