74497-02-2合成路线 (共 11739 条)
反应条件
hexamethylene bis(N-methylimidazolium)bis(dichloroiodate); calcium carbonate in methanol; dichloromethane T=20°C; 0.75 h; regioselective reaction;
参考文献
Nouzarian, Mahboobe; Hosseinzadeh, Rahman; Golchoubian, Hamid
Synthetic Communications, 2013 , vol. 43, # 21 p. 2913 - 2925
反应条件
iodine in benzene 36 h; Irradiation;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 27, # 1-12 p. 154 - 155
参考文献
Hodgson; Marsden
Journal of the Chemical Society, 1937 , p. 1365
参考文献
Michael; Norton
Chemische Berichte, 1878 , vol. 11, p. 109
参考文献
Elbs; Volk
Journal fuer Praktische Chemie (Leipzig), 1919 , vol. <2>99, p. 270
反应条件
1.1: CCl4 / 0 °C 1.2: 40 percent / Ac2O; K10 clay impregnated with copper(II) nitrate / CCl4 / 2 h / 20 °C 2.1: 88 percent / K10; H2 / Pd/C / ethanol / 18 h / 120 °C / 6722.92 Torr View Scheme
参考文献
Fonseca, Tatiana; Gigante, Barbara; Gilchrist, Thomas L
Tetrahedron, 2001 , vol. 57, # 9 p. 1793 - 1799
反应条件
1: 35 percent / sodium nitrate, conc.H2SO4 / 3 h / 0 - 5 °C 2: 58 percent / sodium nitrate, conc. H2SO4 / 3 h / 0 - 5 °C View Scheme
参考文献
Rosevear, Judi; Wilshire, John F. K.
Australian Journal of Chemistry, 1985 , vol. 38, # 5 p. 723 - 733
反应条件
iron(III) trifluoride; iodine in acetonitrile T=80°C; 36 h; Inert atmosphere; regioselective reaction;
参考文献
Fang, Xiao-Li; Tang, Ri-Yuan; Zhang, Xing-Guo; Li, Jin-Heng
Synthesis, 2011 , # 7 p. 1099 - 1105
反应条件
1: With hydrogenchloride; sodium nitrite 2: With hydrogenchloride; tin(ll) chloride
参考文献
Boldyrev, B. G.; Grivnak, L. M.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 2 p. 324 - 330
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 362 - 369
反应条件
in ethanol 2 h; Heating;
参考文献
Aboul-Enein, Hassan Y.; Ibrahim, Said E.
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 233 - 237