74497-02-2合成路线 (共 11739 条)
参考文献
Nippon Kagaku Zasshi, , vol. 80, p. 541,543
Chem.Abstr., , p. 4445
反应条件
AlCl3, aluminium chloride T=100°C; 1 h; Inert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 10, # 2 p. 293 - 304
反应条件
1: zinc chloride / 230 - 240 °C 2: diluted hydrobromic acid / Behandeln der Diazoniumbromid-Loesung mit Kupfer(I)-bromid View Scheme
参考文献
Reilly; Hickinbottom
Journal of the Chemical Society, 1920 , vol. 117, p. 133
反应条件
1: 0.5 h / 150 °C / microwave irradiation 2: 80 percent / 2-Cy2P-2',4',6'-tris(i-Pr)-1,1'-biphenyl; Cs2CO3 / Pd(OAc)2 / toluene / 0.5 h / 100 °C / microwave irradiation View Scheme
参考文献
Poondra, Rajamohan R.; Turner, Nicholas J.
Organic Letters, 2005 , vol. 7, # 5 p. 863 - 866
反应条件
Bu2SnClH-HMPA in tetrahydrofuran T=0°C; 1 h;
参考文献
Shibata, Ikuya; Suwa, Toshihiro; Sugiyama, Erika; Baba, Akio
Synlett, 1998 , # 10 p. 1081 - 1082
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; di-n-butylchlorotin hydride in tetrahydrofuran T=0°C; Reduction; Amination; 1 h;
参考文献
Suwa, Toshihiro; Sugiyama, Erika; Shibata, Ikuya; Baba, Akio
Synthesis, 2000 , # 6 p. 789 - 800
反应条件
in acetonitrile T=80°C; 12 h;
参考文献
Modica; Zanaletti; Freccero; Mella
Journal of Organic Chemistry, 2001 , vol. 66, # 1 p. 41 - 52
反应条件
1: ethanol / 3 h / Reflux 2: sodium tetrahydroborate / methanol / 0.67 h / 0 °C View Scheme
参考文献
Oskooie, Hossein A.; Amiri, Somaih Solemani; Heravi, Majid M.; Ghassemzadeh, Mitra
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2047 - 2050
反应条件
in diphenylether T=260°C; 15 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 522 - 528
参考文献
Paal; Senninger
Chemische Berichte, 1894 , vol. 27, p. 1802