74497-02-2合成路线 （共 11739 条）
参考文献
van Alphen
Recueil des Travaux Chimiques des Pays-Bas, 1932 , vol. 51, p. 179,181
反应条件
Montmorillonite K 10 clay
0.05 h; microwave (800 Watts) irradiation at ca. 110 deg C;
参考文献
Varma, Rajender S.; Dahiya, Rajender
Synlett, 1997 , vol. 1997, # 11 p. 1245 - 1246
反应条件
lithium hydroxide hydrate; Pd/DNA in water
T=50°C; 24 h; Inert atmosphere;
参考文献
Tang, Lin; Sun, Huayin; Li, Yunfeng; Zha, Zhenggen; Wang, Zhiyong
Green Chemistry, 2012 , vol. 14, # 12 p. 3423 - 3428
参考文献
Staudinger; Stockmann
Chemische Berichte, 1909 , vol. 42, p. 3491
参考文献
Wayne; Cohen
Journal of the Chemical Society, 1925 , vol. 127, p. 458
参考文献
Staudinger
Chemische Berichte, 1909 , vol. 42, p. 3976
反应条件
1: 1.) 12 N aq. HCl, aq. NaNO2, 2.) NaOAc, CuCl2*2H2O, 3.) 2,6-lutidine
2: 93 percent / K2CO3 / CH2Cl2 / Irradiation
3: 86 percent / NaAlH2(OCH2CH2OCH3)2 (Vitride-T) / toluene / 1.) RT, 0.5 h, 2.) reflux, 18 h
View Scheme
参考文献
McKenzie, Thomas C.; Epstein, Joseph W.; Fanshawe, William J.; Dixon, J. Scott; Osterberg, Arnold C.; et al.
Journal of Medicinal Chemistry, 1984 , vol. 27, # 5 p. 628 - 632
反应条件
in propan-1-ol
Ambient temperature;
参考文献
Barluenga, Jose; Bayon, Ana M.; Asensio, Gregorio
Journal of the Chemical Society, Chemical Communications, 1983 , # 19 p. 1109 - 1110
反应条件
sodium
3.) r.t., 5 h; Yield given. Multistep reaction;
参考文献
Barluenga, Jose; Bayon, Ana M.; Campos, Pedro; Asensio, Gregorio; Gonzalez-Nunez, Elena; Molina, Yolanda
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1631 - 1636
反应条件
in methanol
Ambient temperature;
参考文献
Barluenga, Jose; Bayon, Ana M.; Asensio, Gregorio
Journal of the Chemical Society, Chemical Communications, 1983 , # 19 p. 1109 - 1110
