N-(2-氨基苯基)-n-环己胺合成路线 (共 7 条)
反应条件
hydrogen; palladium on activated charcoal
参考文献
Chuckowree, Irina; Ali Syed, Murtaza; Getti, Giulia; Parbhu Patel, Asha; Garner, Hannah; Tizzard, Graham J.; Coles, Simon J.; Spencer, John
Tetrahedron Letters, 2012 , vol. 53, # 28 p. 3607 - 3611
反应条件
1: 0.25 h / 170 °C / Microwave irradiation; Neat (no solvent) 2: palladium 10 on activated carbon; hydrogen / ethanol / 20 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 28 p. 3607 - 3611
反应条件
1: palladium diacetate; caesium carbonate; rac-BINAP / toluene / 18 h / 115 °C / |Inert atmosphere 2: hydrogen; palladium on activated charcoal / toluene / 48 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Organometallics, , vol. 32, # 8 p. 2435 - 2442
反应条件
1: potassium carbonate / dimethyl sulfoxide / 17 h / 60 °C 2: palladium(II) oxide hydrate; hydrogen / methanol / 17 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 136, # 12 p. 4551 - 4556
反应条件
sodium hydroxide; borane 1.) THF, RT; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Synthetic Communications, , vol. 14, # 13 p. 1213 - 1220
反应条件
in tetrahydrofuran T=20°C;
参考文献
Zhang, Puwen; Terefenko, Eugene A.; McComas, Casey C.; Mahaney, Paige E.; Vu, An; Trybulski, Eugene; Koury, Elizabeth; Johnston, Grace; Bray, Jenifer; Deecher, Darlene
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 23 p. 6067 - 6070
参考文献
Dannley,R.L.; Grava,A.
Canadian Journal of Chemistry, 1965 , vol. 43, p. 3377 - 3386