3-氯-2-甲基乙酰苯胺合成路线 （共 29 条）
反应条件
in ethanol T=20°C; 2 h;
参考文献
Li, James J.; Hamann, Lawrence; Augeri, David; Bi, Yingzhi
Patent: US2005/197367 A1, 2005 ;
Location in patent: Page/Page column 17 ;
US 20050197367 A1
反应条件
acetic anhydride in acetic acid
反应条件
phosphoric acid Reflux;
参考文献
Bioorganic Chemistry, , vol. 54, p. 31 - 37
参考文献
Journal of the American Chemical Society, , vol. 55, p. 2559,2563
反应条件
1: tin; hydrochloric acid View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 474
反应条件
1: SbCl5; chlorine / <40 2: tin; hydrochloric acid View Scheme
参考文献
Monatshefte fuer Chemie, , vol. 22, p. 474
反应条件
1: conc. HNO3 / acetic anhydride; acetic acid / 2 h / 0 °C 2: NaOCH3 / methanol / 3 h View Scheme
参考文献
Morgan; Glover
Journal of the Chemical Society, 1924 , vol. 125, p. 1598
反应条件
1: potassium permanganate; magnesium sulfate 2: concentrated hydrochloric acid / Zers. des entstandenen Hydrochlorids mit Natriumdicarbonat 3: Diazotization.Einw. von CuCl und HCl auf das Diazotierungsprodukt View Scheme
参考文献
Cohn,P.
Monatshefte fuer Chemie, 1901 , vol. 22, p. 485
反应条件
1: potassium permanganate; magnesium sulfate; water 2: aqueous hydrochloric acid 3: aqueous hydrochloric acid; sodium nitrite / Diazotization.Eintragen der erhaltenen Diazoniumsalz-Loesung in eine aus Kupfer(II)-sulfat, Schwefeldioxid und wss. Ammoniak hergestellte Loesung 4: acetic acid anhydride 5: 310 °C View Scheme
参考文献
Huntress; Cliff
Journal of the American Chemical Society, 1933 , vol. 55, p. 2559,2563
反应条件
1: bromine; acetic acid / 4 h / 0 - 20 °C 2: magnesium sulphate heptahydrate; potassium permanganate / water / 3 h / |Reflux 3: sodium hydroxide / water / 5 h / |Reflux View Scheme
参考文献
Boettcher, Stephan; Hederos, Markus; Champion, Elise; Dekany, Gyula; Thiem, Joachim
Organic Letters, 2013 , vol. 15, # 14 p. 3766 - 3769
