烯丙基-alpha-D-吡喃葡萄糖苷合成路线 (共 12 条)
反应条件
water; acetic acid T=100°C; 1 h;
参考文献
Toyo Suisan Kaisha, Ltd.
Patent: EP2388264 A1, 2011 ;
Location in patent: Page/Page column 40 ;
反应条件
1: allyl alcohol With acetyl chloride T=0°C; 0.5 h; Inert atmosphere; 2: D-glucopyranose T=0 - 70°C; Inert atmosphere;
参考文献
Schindler, Corinna S.; Bertschi, Louis; Carreira, Erick M.
Angewandte Chemie - International Edition, 2010 , vol. 49, # 48 p. 9229 - 9232
反应条件
Dowex 50-X2-100 (H+) 1.5 h; Heating;
参考文献
Jenkins, David J.; Potter, Barry V.L.
Carbohydrate Research, 1996 , vol. 287, # 2 p. 169 - 182
反应条件
Dowex 15 (H+) 2 h; Reflux;
参考文献
Hassan, Hammed H.A.M.
Letters in Organic Chemistry, 2010 , vol. 7, # 2 p. 127 - 135
反应条件
sodium methylate 3 h; Ambient temperature;
参考文献
Carbohydrate Research, , vol. 254, p. 43 - 60
反应条件
Amberlite IR-120 (H+)
参考文献
Journal of the American Chemical Society, , vol. 116, # 17 p. 7919 - 7920
反应条件
gold(III) chloride in acetonitrile 4 h; RefluxInert atmosphere; optical yield given as percent dechemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 74, # 21 p. 8417 - 8420
反应条件
1: tin(IV) chloride / CH2Cl2 / 72 h / 20 °C 2: Et3N; H2O / methanol / 24 h / 20 °C View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 42, # 3 p. 666 - 669
反应条件
trifluoroacetic acid T=105°C; 26 h;
参考文献
Carbohydrate Research, , vol. 342, # 2 p. 217 - 235
参考文献
Tetrahedron Letters, , vol. 47, # 52 p. 9203 - 9206