1H-咪唑-1-二硫代羧酸甲酯合成路线 （共 35 条）
反应条件
1: 1-(methyldithiocarbonyl)imidazole; aniline in ethanol Substitution; Heating; 2: benzylamine in ethanol Substitution; 2.5 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
in ethanol Cyclization; 4.5 h; Heating;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: 1-(methyldithiocarbonyl)imidazole With ammonia in ethanol Substitution; Heating; 2: piperidine in ethanol Substitution; 4.5 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
sodium hydride in tetrahydrofuran; paraffin 1 h; Ambient temperature;
参考文献
Sun, Wei Yan; Hu, Ji Qing; Shi, Yong Ping
Synlett, 1997 , vol. 1997, # 11 p. 1279 - 1280
反应条件
in ethanol Substitution; 4.5 h; Heating;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: in ethanol Substitution; Heating; 2: With ammonia in ethanol Substitution; 4.5 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: in ethanol Substitution; Heating; 2: With ammonia in ethanol Substitution; 5 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: 1-(methyldithiocarbonyl)imidazole; aniline in ethanol Substitution; Heating; 2: morpholine in ethanol Substitution; 6 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: 1-(methyldithiocarbonyl)imidazole; aniline in ethanol Substitution; Heating; 2: phenethylamine in ethanol Substitution; 5.5 h;
参考文献
Mohanta, Pramod K.; Dhar, Sanchita; Samal; Ila; Junjappa
Tetrahedron, 2000 , vol. 56, # 4 p. 629 - 637
反应条件
1: 1H-imidazole With sodium hydride in tetrahydrofuran
T=0°C; 0.416667 h;
2: carbon disulfide in tetrahydrofuran
T=0°C; 0.533333 h;
3: methyl iodide in tetrahydrofuran
T=0°C; 0.666667 h;
参考文献
NOVO NORDISK A/S
Patent: WO2006/3096 A1, 2006 ;
Location in patent: Page/Page column 26-27 ;
WO 2006/003096 A1
