5,6,7,8-四氢-1,4-萘二酮合成路线 （共 16 条）
反应条件
sodium periodate in dichloromethane
T=20°C; 3 h;
参考文献
Gupta, Dharmendra N.; Hodge, Philip; Davies, J. Eric
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2970 - 2973
反应条件
1: 85 percent / RuCl2(PPh3)3 / ethyl acetate; benzene / 4 h / 20 °C
2: 70 percent / TiCl4 / CH2Cl2 / 1.5 h / -78 - 20 °C
3: 61 percent / ceric ammonium nitrate / acetonitrile; H2O / 1 h
View Scheme
参考文献
Mal, Dipakranjan; Ray, Sutapa; Sharma, Indrajeet
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4981 - 4984
反应条件
C96H96Fe2N16O; tetrabutylammonium oxone in dichloromethane
T=20°C; 0.166667 h;
参考文献
Neu, Heather M.; Zhdankin, Viktor V.; Nemykin, Victor N.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6545 - 6548
反应条件
potassium dichromate; sulfuric acid
参考文献
Arnold; Richter
Journal of the American Chemical Society, 1948 , vol. 70, p. 3505
反应条件
1: 1) diazonium salt of sulfanilic acid, 2.) Na2S2O4
2: K2Cr2O7, 5percent aq. H2SO4 / CH2Cl2
View Scheme
参考文献
Kallmayer; Seyfang
Archiv der Pharmazie, 1985 , vol. 318, # 7 p. 607 - 614
反应条件
1: gelatine; aqueous acetic acid; platinum / 50 °C / Hydrogenation
2: acetic acid; aqueous HCl / weiteres Reagens: FeCl3
View Scheme
参考文献
Skita; Rohrmann
Chemische Berichte, 1930 , vol. 63, p. 1473,1484
反应条件
Entzinnung des ausgeschiedenen Zinndoppelsalzes und Oxydation mit Kaliumchromat und verd.Schwefelsaeure;
参考文献
Jacobson; Turnbull
Chemische Berichte, 1898 , vol. 31, p. 898
参考文献
Skita; Rohrmann
Chemische Berichte, 1930 , vol. 63, p. 1473,1484
参考文献
Skita; Rohrmann
Chemische Berichte, 1930 , vol. 63, p. 1473,1484
反应条件
sodium disulfite in diethyl ether; water
Ambient temperaturetime=until decoloration;
参考文献
Malesani, Giorgio; Ferlin, Maria Grazia; Masiero, Sergio
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 633 - 637
