2,3,4,6-四邻乙酰基-alpha-d-吡喃葡萄糖三氯乙酰胺合成路线 （共 68 条）
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane T=-78 - 20°C; Substitution; 0.5 h;
参考文献
Yu, Hai; Yu, Biao; Wu, Xiangyang; Hui, Yongzheng; Han, Xiuwen
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 9 p. 1445 - 1453
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane T=-78 - 20°C; Substitution; 0.5 h;
参考文献
Yu, Hai; Yu, Biao; Wu, Xiangyang; Hui, Yongzheng; Han, Xiuwen
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 9 p. 1445 - 1453
反应条件
4 A molecular sieve; boron trifluoride diethyl etherate in dichloromethane T=-78 - 20°C; Substitution; 0.5 h;
参考文献
Yu, Hai; Yu, Biao; Wu, Xiangyang; Hui, Yongzheng; Han, Xiuwen
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 9 p. 1445 - 1453
反应条件
trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve T=-10°C; Substitution;
参考文献
Yu, Hai; Yu, Biao; Wu, Xiangyang; Hui, Yongzheng; Han, Xiuwen
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 9 p. 1445 - 1453
反应条件
indium(III) chloride in dichloromethane T=30°C; 48 h;
参考文献
Ghosh, Rina; Chakraborty, Arijit; Maiti, Dilip Kumar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2003 , vol. 42, # 3 p. 602 - 604
反应条件
1: in dichloromethane T=0°C; Molecular sieveInert atmosphere; 2: With boron trifluoride diethyl etherate in dichloromethane 3 h; Molecular sieveInert atmosphere;
参考文献
Li, Yali; Mo, Huaping; Lian, Gaoyan; Yu, Biao
Carbohydrate Research, 2012 , vol. 363, p. 14 - 22
反应条件
indium(III) chloride in dichloromethane T=30°C; 4.5 h;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 42, # 3 p. 602 - 604
反应条件
trimethylsilyl trifluoromethanesulfonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=20°C; Title compound not separated from byproducts;
参考文献
Synthesis, , # 13 p. 2074 - 2078
反应条件
Amberlyst 15 in diethyl ether T=20°C; 3 h;
参考文献
Tian, Qiang; Zhang, Shuo; Yu, Qian; He, Mei-Bo; Yang, Jin-Song
Tetrahedron, 2007 , vol. 63, # 10 p. 2142 - 2147
反应条件
trimethylsilyl trifluoromethanesulfonate; 1-n-butyl-3-methylimidazolium hexafluorophosphate T=20°C; Title compound not separated from byproducts;
参考文献
Pakulski, Zbigniew
Synthesis, 2003 , # 13 p. 2074 - 2078
