Kochen des Reaktionsprodukts mit Wasser;

1: K2CO3 / dimethylformamide / 0.17 h / 150 °C 2: 100 percent / conc. HCl, acetic acid / 1 h / Ambient temperature 3: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 4: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 5: pyridine / 2 h / 70 - 80 °C 6: KOH / pyridine / 80 °C 7: 92 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 8: 74 percent / dimethyldioxirane / acetone / 0 °C 9: 85 percent / K2CO3 / acetone / Heating 10: 83 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 11: 88 percent / K2CO3 / methanol / 1.5 h / Heating 12: 89 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme

potassium carbonate in acetone Heating;

Yield given;

暂无反应条件数据

1: potassium-<4-methoxy benzoate> 2: methanol; diethyl ether View Scheme

1: sodium benzoate / 180 °C / Erwaermen des Reaktionsprodukts mit wss.-aethanol. Natronlauge 2: aluminium chloride; nitrobenzene View Scheme

sodium hydroxide Erwaermen des Reaktionsprodukts mit wss.-aethanol. Salzsaeure;

1: K2CO3 / dimethylformamide / 0.17 h / 150 °C 2: 100 percent / conc. HCl, acetic acid / 1 h / Ambient temperature 3: 83 percent / K2CO3, KI / acetone; dimethylformamide / Heating 4: 75 percent / AlBr3, NaI / acetonitrile / 0.25 h / 0 °C 5: pyridine / 2 h / 70 - 80 °C 6: KOH / pyridine / 80 °C 7: 97 percent / conc. H2SO4, acetic acid / 1 h / 50 °C 8: 70 percent / dimethyldioxirane / acetone / 0 °C 9: 81 percent / K2CO3 / acetone / Heating 10: 97 percent / AlCl3 / acetonitrile / 0.5 h / Ambient temperature 11: 96 percent / K2CO3 / methanol / 1.5 h / Heating 12: 74 percent / H2 / 10percent Pd/C / methanol; ethyl acetate / Ambient temperature View Scheme