nBu4NPF6 electrosynthesis: 1.) from -1.10 V to -2.10 V, from 100 mA to 0, irradiation, 2.) -1.6 V, irradiation; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Degrand, Chantal; Prest, Rita; Compagnon, Paul-Louis
Journal of Organic Chemistry, 1987 , vol. 52, # 23 p. 5229 - 5233
Song, Yong-Qi; Yuzuri, Tomoaki; Suezawa, Hiroko; Sakakibara, Kazuhisa; Hirota, Minoru; Nakada, Masahiro
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 8 p. 1875 - 1878
1: With AlCl3, aluminium chloride; boron trichloride in dichloromethane; 1,2-dichloro-ethane T=80°C; Friedel Crafts acylation; 20 h; 2: With hydrogenchloride; water in dichloromethane; 1,2-dichloro-ethane T=80°C; 0.5 h;
参考文献
Jin, Guo Hua; Ha, Sang Keun; Park, Hye Min; Kang, Bomi; Kim, Sun Yeou; Kim, Hee-Do; Ryu, Jae-Ha; Jeon, Raok
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 14 p. 4092 - 4094
