hydrogenchloride; acetone in diethyl ether
HCl passed 5 h into stirred suspn. of Sn in acetone, acetaldehyde and Et2O; ratio of products depended on ratio of educts; filtered, filtrate concd., extd. with cold CHCl3;
参考文献
Burley, Joseph W.; Hope, Peter; Mack, Arthur G.
Journal of Organometallic Chemistry, 1984 , vol. 277, # 1 p. 37 - 46
Pascal, R.; Lasperas, M.; Taillades, J.; Commeyras, A.; Perez-Rubalcaba, A.
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 7-8 p. 329 - 337
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反应条件
zinc in diethyl ether; benzene
0.5 h; Heating; Title compound not separated from byproducts;
参考文献
Khrimyan, A. P.; Makaryan, G. M.; Badanyan, Sh. O.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, p. 81 - 85
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 1 p. 94 - 99
