反应条件
1: diiodomethane With diethylzinc in hexane; dichloromethane T=0°C; 0.166667 h; Inert atmosphere; 2: 4,4-dimethyl-3-oxopentanoic acid methyl ester With iodine; sodium thiosulfate in hexane; dichloromethane; water T=0°C; 0.5 h; 3: With ammonium chloride in hexane; dichloromethane; water
参考文献
Aiken, Karelle S.; Eger, Wilhelm A.; Williams, Craig M.; Spencer, Carley M.; Zercher, Charles K.
Journal of Organic Chemistry, 2012 , vol. 77, # 14 p. 5942 - 5955