dimethyl sulfoxide T=25°C; 2.5 h; Further byproducts given;
参考文献
Maslennikov, E. I.; Talzi, V. P.; Gunbin, V. N.; Yasman, Ya. B.; Gudoshnikov, S. K.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 2258 - 2260
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2558 - 2561
in dichloromethane 1.01 mmol (C5H5)Fe(SMe2)3BF4 and 1.01 mmol Ph2PCH2PPh2 in CH2Cl2 mixed at room temp., mixt. stirred for 5 min, filtrated into Et2O; pptd. Fe complex filtered off, dried in vac.; elem. anal.;
参考文献
Kuhn, Norbert; Schumann, Hans; Winter, Manfred; Zauder, Edgar
Chemische Berichte, 1988 , vol. 121, p. 111 - 116
in dichloromethane 1.01 mmol (C5H5)Fe(SMe2)3BF4 and 2.02 mmol P(OMe)3 in CH2Cl2 mixed at room temp., mixt. stirred for 5 min, filtrated into Et2O; ppt. filtered off, dried in vac.; elem. anal.;
参考文献
Kuhn, Norbert; Schumann, Hans; Winter, Manfred; Zauder, Edgar
Chemische Berichte, 1988 , vol. 121, p. 111 - 116
in dichloromethane 1.01 mmol (C5H5)Fe(SMe2)3BF4 and 1.01 mmol Ph2P(CH2)2PPh2 in CH2Cl2 mixed at room temp., mixt. stirred for 5 min, filtrated into Et2O; pptd. Fe complex filtered off, dried in vac.; elem. anal.;
参考文献
Kuhn, Norbert; Schumann, Hans; Winter, Manfred; Zauder, Edgar
Chemische Berichte, 1988 , vol. 121, p. 111 - 116
in dichloromethane; acetone byproducts: Cl(1-); addn. of (AuCl(SMe2)) in CH2Cl2 to a soln. of Pt-compd. in acetone, stirred for 1 h; volume reduced, addn. of pentane; elem. anal.;
参考文献
Hadj-Bagheri, Nasim; Puddephatt, Richard J.
Inorganica Chimica Acta, 1993 , vol. 213, p. 29 - 40
sodium sulfide; potassium hydroxide in dimethyl sulfoxide T=90 - 100°C; 4 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, # 11 p. 2123 - 2127
Zhurnal Organicheskoi Khimii, , vol. 21, # 11 p. 2324 - 2328
dimethyl sulfoxide T=80°C; 2 h; Further byproducts given;
参考文献
Maslennikov, E. I.; Talzi, V. P.; Gunbin, V. N.; Yasman, Ya. B.; Gudoshnikov, S. K.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 2258 - 2260
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 12 p. 2558 - 2561
