titanium tetrachloride in dichloromethane T=-78°C; 2 h;
参考文献
Ewing, James C.; Ferguson, Gregory S.; Moore, Douglas W.; Schultz, Frederick W.; Thompson, David W.
Journal of Organic Chemistry, 1985 , vol. 50, # 12 p. 2124 - 2128
in N-dodecane excess of Me3Al in dodecane adding to suspn. of anhyd. Zn acetate in dodecane at room temp.; mixt. distg. through a 40 cm vigreux column and product collecting in toluene; identified by b. p.;
参考文献
Ashby, E. C.; Smith, R. Scott
Journal of Organometallic Chemistry, 1982 , vol. 225, # 1 p. 71 - 85
in tetrahydrofuran; diethyl ether; hexane soln. of stannane in THF added to soln. of (Me4Al)Li derived from Me3Al(1.0 M hexane soln.) and MeLi (1.5 M ether soln.) at 0°C, stirred for 40 h at 25°C, workup (1 M HCl, ether); SiO2 column chromy.;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 5 p. 1480 - 1483
hydroxylamine hydrochloride in tetrahydrofuran; toluene T=0°C; Inert atmosphere;
参考文献
Iqbal, Mudassar; Black, Richard J. G.; Winn, Joby; Reeder, Andrew T.; Blake, Alexander J.; Clarke, Paul A.
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 14 p. 5062 - 5078
