反应条件
in tetrahydrofuran
byproducts: C6H8(CH3)(COCH3); AlMe3 in hexanes is added to a soln. of the starting complexes in THF at -10°C under N2, warmed to 25°C, stirred for 30 min; ice is added, the organic layer is dried, the solvent is removed, the oil is chromd.;
参考文献
Wright, Marcus W.; Smalley Jr., Terrence L.; Welker, Mark E.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1994 , vol. 116, # 15 p. 6777 - 6791
