反应条件
hydrogenchloride; n-butyllithium; diisopropylamine in tetrahydrofuran Ar-atmosphere; dropwise addn. of BuLi in THF to diisopropylamine (-78°C), dropwise addn. to B(OMe)3 and C2H4Cl2 in THF, stirring (1 h, -78°C), bubbling of HCl to methyl orange endpoint, dilution with ether; filtration off of iPr2NH*HCl, washing (ether), distn.; elem. anal.;
参考文献
Matteson, Donald S.; Hurst, Gerald D.
Organometallics, 1986 , vol. 5, p. 1465 - 1467
