in diethyl ether
under Ar; soln. of t-BuOH in Et2O added to In compd. (molar ratio 1:1) in Et2O at room temp.; stirred for 1 h; volatiles removed by vac. distn.; recrystd. from Et2O at -40°C; crystals washed with pentane at 0°C; elem. anal.;
参考文献
Beachley Jr.; MacRae, David J.; Churchill, Melvyn Rowen; Kovalevsky, Andrey Yu.; Robirds, Eric S.
Organometallics, 2003 , vol. 22, # 20 p. 3991 - 4000