反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine
1.) pentane, hexane, a) RT, overnight, b) reflux, 24 h, 2.) pentane, hexane, RT, overnight; Yield given. Multistep reaction;
参考文献
Le Roy, Jennifer J.; Jeletic, Matthew; Gorelsky, Serge I.; Korobkov, Ilia; Ungur, Liviu; Chibotaru, Liviu F.; Murugesu, Muralee
Journal of the American Chemical Society, 2013 , vol. 135, # 9 p. 3502 - 3510