反应条件
in dichloromethane
Under inert atmosphere, addn. of Me3SiOTf to an ice-cooled soln. of Ru-complex, a darker yellow color develops, stirring (0°C, 15 min), warming to room temp. (1 h).; Evapn. of volatiles, recrystn. of resulting yellow powder (CH2Cl2/pentane), elem. anal.;
参考文献
Straus, Daniel A.; Zhang, Cheng; Quimbita, Grace E.; Grumbine, Steven D.; Heyn, Richard H.; Tilley, T. Don; Rheingold, Arnold L.; Geib, Steven J.
Journal of the American Chemical Society, 1990 , vol. 112, # 7 p. 2673 - 2681
