in tetrahydrofuran addition of Me3SiCl to a solution of Cp8Ti6N3 in THF and filtration after 5 minutes;; washing with THF and drying in vacuo; IR spectroscopy;;
参考文献
Kilner, Melvyn; Parkin, Gerard
Journal of Organometallic Chemistry, 1986 , vol. 302, # 2 p. 181 - 192