in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -1,3 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of Me3SiCl; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
in ethylene glycol dimethyl ether Electrolysis; (N2); potential controlled electrolysis at -1,6 V (vs. AgI/Ag referenceelectrode) of soln. of Ge compd. at room temp. in presence of Me3SiCl; filtered soln. was evapd. in vac., residue was extd. with ether and solvent removed, residue was sepd. by TLC, products were identified by m. p., IR, NMR and MAS;
参考文献
Corriu, R. J. P.; Dabosi, G.; Martineau, M.
Journal of Organometallic Chemistry, 1980 , vol. 188, # 1 p. 63 - 72
Vasil'eva, T. V.; Stolyarenko, V. Ya.; Yakovleva, G. N.; Yastrebov, V. V.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 11 p. 2570 - 2573,2271 - 2274
