2,2,2-三氟乙醇合成路线 (共 1089 条)
反应条件
8 h; UV-irradiation;
参考文献
Dichiarante, Valentina; Salvaneschi, Andrea; Protti, Stefano; Dondi, Daniele; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 51 p. 15919 - 15926
反应条件
1 h; UV-irradiation;
参考文献
Dichiarante, Valentina; Salvaneschi, Andrea; Protti, Stefano; Dondi, Daniele; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 51 p. 15919 - 15926
反应条件
caesium carbonate; acetone
24 h; UV-irradiationInert atmosphere;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
反应条件
acetone in cyclohexane
UV-irradiation; Quantum yield;
参考文献
Dichiarante, Valentina; Dondi, Daniele; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 17 p. 5605 - 5611
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile
0.25 h;
2: 2,2,2-trifluoroethanol; benzene With caesium carbonate; acetone in acetonitrile
24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile
0.25 h;
2: 2,2,2-trifluoroethanol; allyl-trimethyl-silane With caesium carbonate; acetone in acetonitrile
24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
反应条件
acetone in cyclohexane
UV-irradiation; Quantum yield;
参考文献
Dichiarante, Valentina; Dondi, Daniele; Protti, Stefano; Fagnoni, Maurizio; Albini, Angelo
Journal of the American Chemical Society, 2007 , vol. 129, # 17 p. 5605 - 5611
反应条件
1: 4-methoxy-phenol With nonafluoro-n-butanesulfonyl fluoride; caesium carbonate in acetonitrile
0.25 h;
2: 3-vinylpropionic acid; 2,2,2-trifluoroethanol With caesium carbonate; acetone in acetonitrile
24 h; Inert atmosphereUV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708
参考文献
Canning, Peter S. J.; Maskill, Howard; McCrudden, Katharine; Sexton, Brian
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 4 p. 789 - 800
反应条件
caesium carbonate; acetone
24 h; UV-irradiation;
参考文献
Raviola, Carlotta; Canevari, Veronica; Protti, Stefano; Albini, Angelo; Fagnoni, Maurizio
Green Chemistry, 2013 , vol. 15, # 10 p. 2704 - 2708