反应条件
1.1: trichlorophosphate / 0 °C / Heating 1.2: 4 h / 55 - 75 °C 1.3: 3 h / 20 °C 2.1: sodium sulfide / N,N-dimethyl-formamide; water / 0.25 h / 20 °C 2.2: 1.5 h / 20 °C 2.3: 1 h 3.1: potassium hydroxide; water / methanol / 3 h / Reflux 3.2: pH 3 View Scheme
参考文献
Dumas, Jacques; Khire, Uday; Lowinger, Timothy B.; Paulsen, Holger; Riedl, Bernd; Scott, William J.; Smith, Roger A.; Wood, Jill; Hatoum-Mokdad, Holia; Lee, Wendy; Redman, Aniko; Johnson, Jeffrey; Sibley, Robert
Patent: US2012/46290 A1, 2012 ;
US 20120046290 A1