hydrogenchloride in tetrahydrofuran; diethyl ether
byproducts: H2; 2,3-dimethyl-2-butene added to a soln. of BH3*(CH3)2S in THF maintaining the temp. below 10°C; stirred for 1 h at 25°C; treated with an ethereal soln. of HCl at 0-5°C;
参考文献
Zweifel, George; Pearson, Norman R.
Journal of the American Chemical Society, 1980 , vol. 102, # 18 p. 5919 - 5920