1-碘-2,5-二甲氧基-4-甲基苯合成路线 (共 7 条)
反应条件
sulfuric acid; iodine; iodic acid in water; acetic acid T=70°C; 12 h;
参考文献
Lucht, Brett L.; Mao, Shane S. H.; Tilley, T. Don
Journal of the American Chemical Society, 1998 , vol. 120, # 18 p. 4354 - 4365
反应条件
copper(l) iodide in N,N-dimethyl acetamide; toluene T=152 - 153°C; Yield given. Yields of byproduct given;
参考文献
European Journal of Organic Chemistry, , # 2 p. 335 - 348
参考文献
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, , vol. 143, p. 196,197
Chem. Zentralbl., , vol. 105, # I p. 3054
反应条件
nitric acid; acetic acid T=45°C;
参考文献
Gilman et al.
Journal of the American Chemical Society, 1944 , vol. 66, p. 798,800
参考文献
Gilman et al.
Journal of the American Chemical Society, 1944 , vol. 66, p. 798,800
反应条件
Pd0(tris(tert-butyl)phosphine)2; α-cyclohexylcyclohexanemethanamine; lithium chloride in 1,4-dioxane T=110°C;
参考文献
Kohrt, Jeffrey T.; Conn, Ed; Maguire, Robert; Wright, Stephen W.; Singer, Robert
Tetrahedron Letters, 2013 , vol. 54, # 51 p. 7065 - 7068
反应条件
copper T=210 - 245°C;
参考文献
Erdtman
Proceedings of the Royal Society of London, Series A: Mathematical, Physical and Engineering Sciences, 1934 , vol. 143, p. 196,197
Chem. Zentralbl., 1934 , vol. 105, # I p. 3054