2,3,4,6-四甲氧基苯乙酮合成路线 （共 22 条）
参考文献
Gardner et al.
Journal of the American Chemical Society, 1956 , vol. 78, p. 2541
反应条件
aluminium trichloride in diethyl ether
T=22°C; 2 h;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
反应条件
potassium carbonate in acetone
10 h; Heating;
参考文献
Tanaka, Nobutoshi; Yamazaki, Naomi; Hori, Kazuyuki; Murakami, Takao; Saiki, Yasuhisa; Chen, Chiu-Ming
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 4 p. 1355 - 1358
反应条件
In(OSO2CF3)3
T=75 - 90°C; 0.1 h; microwave irradiation;
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
反应条件
potassium hydroxide in ethanol
7 h; Heating;
参考文献
Tanaka, Nobutoshi; Yamazaki, Naomi; Hori, Kazuyuki; Murakami, Takao; Saiki, Yasuhisa; Chen, Chiu-Ming
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, # 4 p. 1355 - 1358
反应条件
(i) aq. KOH, EtOH, (ii) (methylation); Multistep reaction;
参考文献
ApSimon,J.W. et al.
Journal of the Chemical Society, 1963 , p. 3780 - 3782
参考文献
Chapman; Perkin; Robinson
Journal of the Chemical Society, 1927 , p. 3020
Show Details
Bargellini; Bini
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1910 , vol. <5> 19 II, p. 598
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 17
反应条件
1: 2.85 g / AlCl3 / acetonitrile / 1 h / 70 °C
2: 59 percent / aq. NaOH; aq. H2O2 / methanol / 2 h / 3 - 20 °C
3: 7.52 g / K2CO3 / acetone / 1.5 h / 60 °C
4: 75 percent / In(CF3SO3)3 / 0.25 h / microwave irradiation
View Scheme
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
参考文献
Cavell,B.D.; MacMillan,J.
Journal of the Chemical Society [Section] C: Organic, 1967 , vol. <C>, p. 310 - 313
反应条件
aluminium trichloride in acetonitrile
0.025 h; HeatingMicrowave irradiation;
参考文献
Tsukayama, Masao; Kusunoki, Eiji; Hossain, Mohammad M.; Kawamura, Yasuhiko; Hayashi, Shinji
Heterocycles, 2007 , vol. 71, # 7 p. 1589 - 1600
