1,2,3,4-四苯基萘合成路线 (共 86 条)
反应条件
tris(dibenzylideneacetone)dipalladium (0); 18-crown-6 ether; cesium fluoride in toluene Ambient temperature;
参考文献
Journal of the American Chemical Society, , vol. 121, # 24 p. 5827 - 5828
反应条件
copper diacetate; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in N,N-dimethyl-formamide 2 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 72, # 14 p. 5362 - 5367
反应条件
pyridine; sodium hexachloropalladate(IV) tetrahydrate; copper (II) acetate monohydrate; silver nitrate in acetonitrile T=110°C; 36 h; Inert atmosphere;
参考文献
Wu, Yao-Ting; Huang, Ke-Hsin; Shin, Chien-Chueh; Wu, Tsun-Cheng
Chemistry - A European Journal, 2008 , vol. 14, # 22 p. 6697 - 6703
反应条件
tetrabutylammomium bromide; potassium carbonate; palladium diacetate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=100°C; 72 h;
参考文献
Journal of Organometallic Chemistry, , vol. 555, # 1 p. 141 - 144
反应条件
in benzene T=70°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 27, # 42 p. 5105 - 5108
反应条件
anhydrous lithium acetate; palladium diacetate; lithium chloride in N,N-dimethyl-formamide T=100°C; 6 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 4 p. 631 - 636
反应条件
tetrabutyl ammonium fluoride in dichloromethane Ambient temperature;
参考文献
Kitamura, Tsugio; Yamane, Masakatsu
Journal of the Chemical Society, Chemical Communications, 1995 , # 9 p. 983 - 984
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene heating soln. of Ge-compd. and catalyst in toluene (70°C), bubbling HCCH into soln. (3 h); chromy. (silica gel, hexane) or destn. (80-90°C, 0.04 Torr); MS;
参考文献
Organometallics, , vol. 9, # 3 p. 869 - 871
参考文献
Journal of the Chemical Society, Chemical Communications, , # 14 p. 787 - 788
反应条件
in cyclohexane Irradiation (UV/VIS); irradn. with a low-pressure mercury lamp (254 nm) for 5h at room temp.; distn. under reduced pressure, purifn. by GLC;
参考文献
Ando, Wataru; Itoh, Hiroyuki; Tsumuraya, Takeshi
Organometallics, 1989 , vol. 8, p. 2759 - 2766