1,2,3,4-四苯基萘合成路线 （共 86 条）
反应条件
in solid matrix Irradiation (UV/VIS); quartz UV cell, degassing by three freeze-pump-thaw cycles, placing the cell into a quartz windowed Dewar filled with liquid N2, irradn. with a low-pressure mercury lamp (254 nm) at 77K for 5-30min., warming to room temp., recooling to 77K, 3-MP matrix; not isolated, detd. by UV;
参考文献
Organometallics, , vol. 8, p. 2759 - 2766
反应条件
silver(I) acetate in para-xylene; acetonitrile T=110°C; 36 h;
参考文献
Wu, Yao-Ting; Huang, Ke-Hsin; Shin, Chien-Chueh; Wu, Tsun-Cheng
Chemistry - A European Journal, 2008 , vol. 14, # 22 p. 6697 - 6703
反应条件
methyloxirane in 1,2-dichloro-ethane Heating;
参考文献
Nakayama, Juzo; Kuroda, Masami; Hoshino, Masamatsu
Heterocycles, 1986 , vol. 24, # 5 p. 1233 - 1236
反应条件
copper diacetate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in o-xylene Heating;
参考文献
Journal of Organic Chemistry, , vol. 73, # 1 p. 298 - 300
反应条件
copper diacetate; [RhCl(η2:η2-cycloocta-1,5-diene)]2 in o-xylene Heating;
参考文献
Journal of Organic Chemistry, , vol. 73, # 1 p. 298 - 300
反应条件
silver(I) acetate; palladium diacetate in acetonitrile T=110°C; 36 h; Inert atmosphere;
参考文献
Wu, Yao-Ting; Huang, Ke-Hsin; Shin, Chien-Chueh; Wu, Tsun-Cheng
Chemistry - A European Journal, 2008 , vol. 14, # 22 p. 6697 - 6703
反应条件
bromine in tetrachloromethane 0 to 20 deg C;
参考文献
Appler, Hubertus; Neumann, Wilhelm P.
Journal of Organometallic Chemistry, 1986 , vol. 314, p. 247 - 260
反应条件
in benzene-d6 T=20°C; 38 h; Inert atmosphereUV-irradiation;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 9-10 p. 1419 - 1426
反应条件
bis(acetylacetonato) palladium; silver(I) acetate in o-xylene T=140°C; Heck reaction; 1 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 9 p. 1431 - 1436
反应条件
in benzene all manipulations under dry Ar; heating benzene soln. of 2,3-benzo-7,7-dimethyl-1,4,5,6-tetraphenyl-7-germanorborna-2,5-diene and bis(trimethylsilyl)thioketene (70°C, 3 h); preparative GLC (10percent SF-96 on Celite 545);
参考文献
Organometallics, , vol. 8, p. 1467 - 1472
