1,2,3,4-四苯基萘合成路线 （共 86 条）
反应条件
in benzene 20 h; Heating;
参考文献
Barton, Derek H. R.; Finet, Jean-Pierre; Motherwell, William B.; Pichon, Clotilde
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 251 - 260
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; copper (II) acetate monohydrate in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Fukutani, Tatsuya; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Journal of Organic Chemistry, 2011 , vol. 76, # 8 p. 2867 - 2874
反应条件
1: With 1,10-phenanthroline; iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane in tetrahydrofuran T=0°C; 1 h; Inert atmosphereSchlenk technique; 2: With hydrogenchloride in tetrahydrofuran; water
参考文献
Ilies, Laurean; Matsumoto, Arimasa; Kobayashi, Motoaki; Yoshikai, Naohiko; Nakamura, Eiichi
Synlett, 2012 , vol. 23, # 16 art. no. ST-2012-U0548-L, p. 2381 - 2384
反应条件
(i) N2O3, CH2Cl2, (ii) /BRN= 471803/, THF; Multistep reaction;
参考文献
Tetrahedron, , vol. 31, p. 1391 - 1398
反应条件
in tetrachloromethane T=70°C;
参考文献
Tetrahedron Letters, , vol. 21, p. 3273 - 3276
反应条件
in benzene all manipulations under dry Ar; heating soln. of di-tert-butylthioketene and 2,3-benzo-7,7-dimethyl-1,4,5,6-tetraphenyl-7-germanorborna-2,5-diene in benzene (70°C, 2.5 h); preparative GLC (10percent SF-96 on Celite 545);
参考文献
Ando, Wataru; Tsumuraya, Takeshi
Organometallics, 1989 , vol. 8, p. 1467 - 1472
反应条件
T=250°C; 2 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 9-10 p. 1419 - 1426
反应条件
in tetrachloromethane 20 h reflux (Ar); distn., column chromy.;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry, , p. 251 - 259
反应条件
anhydrous lithium acetate; palladium diacetate; lithium chloride in N,N-dimethyl-formamide T=100°C; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 4 p. 631 - 636
反应条件
in methanol; benzene T=540°C;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 14 p. 787 - 788
