1,2,3,4-四苯基萘合成路线 (共 86 条)
反应条件
triglyme (triethylene glycol dimethyl ether)
参考文献
Grein, Kornelia; Kirste, Burkhard; Kurreck, Harry
Chemische Berichte, 1981 , vol. 114, # 1 p. 254 - 266
参考文献
Luis, Santiago V.; Ferrer, Patrick; Burguete, M. Isabel
Journal of Organic Chemistry, 1990 , vol. 55, # 12 p. 3808 - 3812
参考文献
Ando, Wataru; Hamada, Yoshitaka; Sekiguchi, Akira
Journal of the Chemical Society, Chemical Communications, 1982 , # 14 p. 787 - 788
反应条件
n-Bu4Br; water; potassium carbonate; palladium diacetate in N,N-dimethyl-formamide T=100°C; 72 h; other reag.; other catalyst; other solvent; Product distribution;
参考文献
Journal of Organometallic Chemistry, , vol. 555, # 1 p. 141 - 144
反应条件
in benzene T=70°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 27, # 42 p. 5105 - 5108
反应条件
in benzene T=70°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 27, # 42 p. 5105 - 5108
反应条件
CCl4 in toluene Kinetics; At 70-90°C 7-germabenzonorbornadiene-compound is added to CCl4, filled under argon into the NMR tube, and heated in a thermostat for 3 h, thermal decompn.,; GC analysis demonstrates the presence of C2Cl6 and Me2GeCl2 in yields of 100 percent and 95 percent, Me2ClGeCCl3 is detected by (1)H NMR, tetraphenylnaphthalene is pptd. with EtOH (quant. yield);
参考文献
Organometallics, , vol. 7, p. 1201 - 1207
反应条件
T=180°C; 1 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 9-10 p. 1419 - 1426
反应条件
T=250°C; 2 h; Inert atmosphere;
参考文献
Journal of Organometallic Chemistry, , vol. 694, # 9-10 p. 1419 - 1426
反应条件
1: With 1,10-phenanthroline; iron (III) acetylacetonate; 1,2-dichloro-2-methylpropane in tetrahydrofuran T=0°C; 1 h; Inert atmosphereSchlenk technique; 2: With hydrogenchloride in tetrahydrofuran; water Catalytic behavior; Reagent/catalyst;
参考文献
Synlett, , vol. 23, # 16 art. no. ST-2012-U0548-L, p. 2381 - 2384