4-乙酰氧基-联苯-4-羧酸合成路线 （共 8 条）
反应条件
sodium hydroxide in ethanol; water Hydrolysis; Heating;
参考文献
Brilev, V. V.; Vasilevskii, D. A.; Tarasevich, V. A.; Matveenko, Yu. V.; Erdman, A. A.
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, 1999 , vol. 69, # 1 p. 126 - 129
反应条件
sulfuric acid
T=80°C; 4 h;
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.
Patent: EP1380567 A1, 2004 ;
Location in patent: Page 5 ;
反应条件
sulfuric acid; acetic anhydride in water
参考文献
Mitsubishi Gas Chemical Co., Inc.
Patent: US2003/124268 A1, 2003 ;
反应条件
sulfuric acid
T=80°C; 4 h;
参考文献
Mitsubishi Gas Chemical Co., Inc.
Patent: US6677475 B2, 2004 ;
Location in patent: Page column 10 ;
反应条件
sodium bromide; zirconium monoxide; manganese; cobalt in acetic anhydride; acetic acid
T=105°C; Oxidation; 4 h;
参考文献
Brilev, V. V.; Vasilevskii, D. A.; Tarasevich, V. A.; Matveenko, Yu. V.; Erdman, A. A.
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, 1999 , vol. 69, # 1 p. 126 - 129
反应条件
2: 76 percent / NaBr / Co-Mn-ZrO / acetic acid; acetic anhydride / 3.5 h / 105 °C
View Scheme
参考文献
Brilev, V. V.; Vasilevskii, D. A.; Tarasevich, V. A.; Matveenko, Yu. V.; Erdman, A. A.
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, 1999 , vol. 69, # 1 p. 126 - 129
反应条件
1: Pd/C / 270 - 310 °C
3: 76 percent / NaBr / Co-Mn-ZrO / acetic acid; acetic anhydride / 3.5 h / 105 °C
View Scheme
参考文献
Brilev, V. V.; Vasilevskii, D. A.; Tarasevich, V. A.; Matveenko, Yu. V.; Erdman, A. A.
Russian Journal of General Chemistry, 1999 , vol. 69, # 1 p. 122 - 125
Zhurnal Obshchei Khimii, 1999 , vol. 69, # 1 p. 126 - 129
反应条件
acetic acid; sodium bromide; anhydrous cobalt diacetate; Manganese (II) acetate
1.) 110 deg C, 60 min, 2.) 105 deg C;
参考文献
Koshel'; Voronenkov; Rudkovskii; Krestinina
Russian Journal of Organic Chemistry, 1997 , vol. 33, # 7 p. 1044 - 1045
