sodium hydroxide; tetra(n-butyl)ammonium hydroxide in dichloromethane 1.5 h; Ambient temperature;

1: 4-methoxyphenyl picolinate With palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in toluene T=115°C; 0.166667 h; 2: butyraldehyde With tert.-butylhydroperoxide in toluene 48 h; Reflux;

1.1: 4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / tetrahydrofuran / 25 °C 2.1: palladium diacetate; 1,2-bis-(diphenylphosphino)ethane / toluene / 0.17 h / 115 °C 2.2: 48 h / |Reflux View Scheme

暂无反应条件数据

1: 1) 60percent AlCl3 / 3 h / 150 °C 2: 88 percent / pyridine / 0.25 h / Ambient temperature View Scheme