反应条件
n-butyllithium; chloro-trimethyl-silane; ammonium chloride in tetrahydrofuran; dichloromethane; Petroleum ether Ar; nBuLi, indene, petroleum ether, -10°C; stirring, room temp.; ppt. dissolved in THF; Me3SiCl in THF added; stirring, room temp., 6 h; aq. NH4Cl added, 0°C; extd. with Et2O; evapn.; dissolved in CH2Cl2; TiCl4/CH2Cl2 added, stirring; solvent removed under vac., residue washed with petroleum ether, dried; elem. anal.;
参考文献
Polo, Eleonora; Barbieri, Andrea; Traverso, Orazio
New Journal of Chemistry, 2004 , vol. 28, # 5 p. 652 - 656