in neat (no solvent) byproducts: SiBr4; distillation of a solution of I2 and SiBr4 or passing the mixture in a H2 stream to crystalline Si near red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
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Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) The halogen was co-condensed in a flask at -196°C with the mixt. of SiF4 and SiF2 emerging out of the reactor tube;; evapd.,; the volatile products were sepd. and detected by NMR and MS;;
参考文献
Suresh, Bettadapura S.; Thompson, James Charlton
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1987 , p. 1123 - 1126
Orndorff; Terrasse; Morton
American Chemical Journal, 1897 , vol. 19, p. 863
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Will; Rhodius
Justus Liebigs Annalen der Chemie, 1848 , vol. 65, p. 230
Orndorff; Terrasse; Morton
American Chemical Journal, 1897 , vol. 19, p. 863
Full Text Show Details
Will; Rhodius
Justus Liebigs Annalen der Chemie, 1848 , vol. 65, p. 230
