on distilling of compd. on iodine and storing at room temp.;; about half of amt. (compd.) is still unchanged, some amt. is reacting to Cl3SII and a black ppt. is resting (distn. not possible);;
in neat (no solvent) heating of SiHCl3 and I2 in a melting tube at 200 -250°C;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 611 - 614
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) reaction in a melting tube at about 200-250°C;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
