in chloroform
N2; room temp.;; neutralized with sodium thiosulphate; solvent removed;;
参考文献
Plooy, Karen E. du; Marais, Charles F.; Carlton, Laurence; Hunter, Roger; Boeyens, Jan C. A.; Coville, Neil J.
Inorganic Chemistry, 1989 , vol. 28, p. 3855 - 3860
in dichloromethane
byproducts: I(CH2)5I; under N2: dissoln. of heterobimetallic Fe/W complex in CH2Cl2; addn. of soln. of I2 in CH2Cl2 at 0°C; stirring, 0°C, 10min;; evapn. (vac.); dissoln. in CH2Cl2; transferring to an alumina column: elution with hexane (two yellow bands) and CH2Cl2-hexane (10percent, yellow soln.); evapn. of solvents; detn. of mixt. of Fe and Ru complex by IR, 1H-NMR, of trace of I(CH2)5I by 1H-NMR;;
参考文献
Friedrich, Holger B.; Moss, John R.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1993 , # 19 p. 2863 - 2870
