water neutralization of destillated HI with KHCO3, evaporation; product free from chloride, iodate and sulfate;
参考文献
Pettenkofer, M.
Liebigs Annalen der Chemie, 1866 , vol. 138, p. 57
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Gmelin Handbook: K: MVol.3, 2.1.1.1, page 586 - 588
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反应条件
in acetonitrile immersing lithiated ferrite in 0.1 M iodine acetonitrile soln. for 5 days at 60°C; washing sample with acetonitrile, drying for 1 h at 120°C in air;atomic absorption spectroscopy anal.;
参考文献
Ito; Omomo; Fujii
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 2 p. 317 - 321
Potylizyn
Ber. Dtsch. Chem. Ges., 1887 , vol. 20, p. 772 - 772
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Gmelin Handbook: Cl: MVol., 118, page 316 - 318
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反应条件
in acetonitrile immersing lithiated ferrite in 0.1 M iodine acetonitrile soln. for 5 days at 60°C; washing sample with acetonitrile, drying for 1 h at room temp. in vac.; atomic absorption spectroscopy anal., X-ray diffraction anal.;
参考文献
Ito; Omomo; Fujii
Bulletin of the Chemical Society of Japan, 2001 , vol. 74, # 2 p. 317 - 321
Emeleus, H. J.; MacDuffie, D. E.
Journal of the Chemical Society, 1961 , p. 2597 - 2599
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Gmelin Handbook: Ag: MVol.B7, 1.20.2.1.1, page 4 - 10
