反应条件
in nitric acid byproducts: nitrous gases; addn. of 5-fold excess of fuming HNO3 to finely dispersed I2 in Erlenmeyer flask closed with glass funnel and round flask with flowing water; heating to 70-80°C on bath of metal chips; arising temp. with time of reaction;; decanting; washing residue with water several times, evapn. to dryness;;
参考文献
Baxter, G. P.; Tilley, G. St.
Z. Anorg. Chem., 1909 , vol. 61, p. 295 - 295
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Baxter, G. P.; Tilley, G. St.
Journal of the American Chemical Society, 1909 , vol. 31, p. 202 - 202
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Gmelin Handbook: I: MVol.2, 104, page 471 - 473