N,N-二甲基硫代甲酰胺合成路线 （共 52 条）
反应条件
1: T=60°C; 3 h; 2: in xylene T=20°C; 22 h; Heating / reflux;
参考文献
WO2005/28445 A2, ;
Page/Page column 27-28 ;
WO 2005/028445 A2
反应条件
triethylamine; triphenylphosphine in dichloromethane
参考文献
Kozmin, Sergey A.; Rawal, Viresh H.
Journal of Organic Chemistry, 1997 , vol. 62, # 16 p. 5252 - 5253
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether; cyclohexane T=-78 - 20°C; 2: ethylmagnesium bromide in tetrahydrofuran; diethyl ether; cyclohexane T=20°C; 2 h;
参考文献
Murai, Toshiaki; Asai, Fumio
Journal of the American Chemical Society, 2007 , vol. 129, # 4 p. 780 - 781
反应条件
silver trifluoroacetate; triethylamine in acetonitrile 1 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 67, # 11 p. 3048 - 3052
反应条件
lithium diisopropyl amide in tetrahydrofuran; diethyl ether; hexane T=-78°C; 2 h;
参考文献
Creary, Xavier; Hatoum, Holia N.; Barton, Angela; Aldridge, Timothy E.
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1887 - 1897
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Murai, Toshiaki; Matsushita, Koji
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 5 p. 1094 - 1103
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 5 p. 1094 - 1103
反应条件
pyridine; disulfur dichloride in dichloromethane
参考文献
Walter,W.; Becker,R.F.
Justus Liebigs Annalen der Chemie, 1972 , vol. 755, p. 145 - 162
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Murai, Toshiaki; Matsushita, Koji
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 5 p. 1094 - 1103
反应条件
1: N,N-dimethyl-thioformamide; phenyllithium in diethyl ether T=-78 - 20°C; 1 h; 2: dimethyl zinc in diethyl ether T=0 - 20°C; 6 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 186, # 5 p. 1094 - 1103
