758640-21-0合成路线 (共 138 条)
参考文献
Chemische Berichte, , vol. 48, p. 1694
反应条件
sulfur in neat (no solvent) T=140°C; 20 h; Inert atmosphere; Temperature;
参考文献
Nguyen, Thanh Binh; Ermolenko, Ludmila; Dean, William A.; Al-Mourabit, Ali
Organic Letters, 2012 , vol. 14, # 23 p. 5948 - 5951
反应条件
1.1: boron trichloride / benzene / Cooling with ice 1.2: Reflux 2.1: morpholine; potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; trimethylphosphane / N,N-dimethyl-formamide; chlorobenzene / 48 h / 100 °C / Inert atmosphere View Scheme
参考文献
Ueno, Satoshi; Shimizu, Ryosuke; Maeda, Ryohei; Kuwano, Ryoichi
Synlett, 2012 , vol. 23, # 11 p. 1639 - 1642
反应条件
1.1: boron trichloride / benzene / Cooling with ice 1.2: Reflux 2.1: potassium phosphate; [Ni0(1,5-cyclooctadiene)2]; trimethylphosphane / N,N-dimethyl-formamide; chlorobenzene / 48 h / 100 °C / Inert atmosphere View Scheme
参考文献
Ueno, Satoshi; Shimizu, Ryosuke; Maeda, Ryohei; Kuwano, Ryoichi
Synlett, 2012 , vol. 23, # 11 p. 1639 - 1642
反应条件
sodium acetate T=150°C;
参考文献
Bischoff
Chemische Berichte, 1898 , vol. 31, p. 2674
反应条件
1: With Y[N(Si(methyl)3)2]3(μ-Cl)Li(tetrahydrofuran)3 in tetrahydrofuran T=20°C; 0.25 h; Inert atmosphere; 2: T=20°C; 0.333333 h;
参考文献
Zhang, Lijun; Xia, Jing; Li, Qinghai; Li, Xihong; Wang, Shaowu
Organometallics, 2011 , vol. 30, # 3 p. 375 - 378
反应条件
nickel sulphate; sodium hydroxide; dipotassium peroxodisulfate in dichloromethane; water 24 h; Ambient temperature;
参考文献
Yamazaki, Shigekazu
Chemistry Letters, 1992 , # 5 p. 823 - 826
反应条件
copper(l) chloride in acetic acid Heating;
参考文献
Shawcross, Andrew P.; Stanforth, Stephen P.
Tetrahedron, 1988 , vol. 44, # 5 p. 1461 - 1464
反应条件
4-(N,N-dimethlyamino)pyridine in chloroform T=20°C; 16 h;
参考文献
Alvarez-Perez, Monica; Goldup, Stephen M.; Leigh, David A.; Slawin, Alexandra M. Z.
Journal of the American Chemical Society, 2008 , vol. 130, # 6 p. 1836 - 1838
参考文献
Badr,M.Z.A.; El-Sherief,H.A.H.
Canadian Journal of Chemistry, 1975 , vol. 53, p. 3831 - 3836