in further solvent(s) to suspn. of Os complex in tetraglyme transferred in vac. CF3COOH (molar ratio 1:1), mixt. stirred at room temp. for 2 h, 2 equiv FSO3C2H5 distd. into react. vessel, mixt. stirred at room temp. for 5 min; mixt. of product and CF3COOCH3 distd. into -196°C cold trap, redistd. into -56°C trap, fractionated on vac. line (in -23°Ctrap);
参考文献
Carter, Willie J.; Kelland, John W.; Okrasinski, Stanley J.; Warner, Keith E.; Norton, Jack R.
Inorganic Chemistry, 1982 , vol. 21, p. 3955 - 3960
