oxygen in toluene addn. of quinone in toluene to Ph3CCl (20°C), treatment (1 h), sepn. of Hg, passing of oxygen through soln., pptn.; further product; sepn. of trityl peroxide (filtration off), removal of toluene, addn. ofhexane, pptn. of Ph2Hg; PhMe2SiCl and further product in mother liquor not isolated; GLC;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, p. 1888 - 1893
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2138 - 2144
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 31, p. 1888 - 1893
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 9 p. 2138 - 2144
1: pyridine / 0.5 h / steam bath 2: 85 percent / pyridine / 32 h / Ambient temperature 3: 89 percent / NaOH / ethanol / 1 h / Heating View Scheme
参考文献
Herdewijn, Piet; Bruyn, Andre De; Wigerinck, Piet; Hendrix, Chris; Kerremans, Luk; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 3 p. 249 - 256
