in tetrahydrofuran Electrochem. Process; electroreduction, 3 F/mol electricity based on Me3GeCl, presence of LiClO4, molar ratio 1:2, Mg cathode and anode, sonication;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 12 p. 896 - 897
methyl-magnesium iodide in diethyl ether (C6H5)3SiCl and an excess of CH3MgI in ether; evapn. of the ether; heating of the residue at 130°C for a few hours;;