3-甲基-3-丁烯-1-醇合成路线 （共 220 条）
反应条件
Montmorillonite K10 T=20°C; 216 h;
参考文献
Desaubry, Laurent; Nakatani, Yoichi; Ourisson, Guy
Tetrahedron Letters, 2003 , vol. 44, # 36 p. 6959 - 6961
反应条件
1: montmorillonite K 10 / 216 h / 20 °C 2: montmorillonite K10 / 216 h / 20 °C View Scheme
参考文献
Desaubry, Laurent; Nakatani, Yoichi; Ourisson, Guy
Tetrahedron Letters, 2003 , vol. 44, # 36 p. 6959 - 6961
反应条件
1: benzene / Ambient temperature 2: 76 percent / pyridine / benzene / 1 h 3: 99 percent / n-Bu3SnH, AIBN / benzene / Heating; other Se-phenyl selenocarbonates; other solvent; other reaction time; regioselectivity; synthesis of γ- and δ-lactones View Scheme
参考文献
Ueki, Yusuke; Ito, Hideto; Usui, Ippei; Breit, Bernhard
Chemistry - A European Journal, 2011 , vol. 17, # 31 p. 8555 - 8558
反应条件
1: 86 percent / Jones reagent / acetone / 1 h / 0 °C 2: SOCl2 / 4 h View Scheme
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
1: 2-methyl-4-hydroxy-1-butene With sodium hydride in triglyme (triethylene glycol dimethyl ether) 2: methyl iodide
参考文献
Bowen, Richard D.; Edwards, Howell G.M.; Varnali, Tereza
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2012 , vol. 93, p. 26 - 32
反应条件
anhydrous lithium acetate; tetrabutyl-ammonium chloride; lithium chloride; palladium diacetate in N,N-dimethyl-formamide T=50°C; 84 h;
参考文献
Larock; Leung; Stolz-Dunn
Tetrahedron Letters, 1989 , vol. 30, # 48 p. 6629 - 6632
反应条件
diethyl azodicarboxylic acid ester; triphenylphosphine in tetrahydrofuran; toluene T=20°C; 1 h; Heating / reflux;
参考文献
CHUGAI SEIYAKU KABUSHIKI KAISHA
Patent: EP1174424 A1, 2002 ;
Location in patent: Page 9 ;
反应条件
water; titanium tetrachloride 1.) diethyl ether, 25 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Moret, Etienne; Schlosser, Manfred
Tetrahedron Letters, 1985 , vol. 26, # 37 p. 4423 - 4426
反应条件
1: 86 percent / Jones reagent / acetone / 1 h / 0 °C 2: SOCl2 / 4 h 3: diethyl ether 4: 73 percent / boron trifluoride etherate / CH2Cl2 / 2 h / 0 °C View Scheme
参考文献
Smith,A.B.; Toder,B.H.; Branca,S.J.
Journal of the American Chemical Society, 1981 , vol. 103, p. 1996
反应条件
hydrogen; RhH(CO)(triphenylphosphine)3; dicobalt octacarbonyl in 1,4-dioxane T=100°C; P=100 Torr; 12 h;
参考文献
Hirai, Kenji; Fujita, Makoto; Fuchikami, Takamasa
Journal of Organometallic Chemistry, 1985 , vol. 279, p. 203 - 214
